Patents

IN192392: A process for the preparation of nanosized hydroxyapatite

A process for the preparation of nanosized hydroxyapatite, which comprises; i) mixing calcium nitrate solution of strength 0.2-0.4 M and ammonium hydroxide solution of strength ranging between 3 to 5M in a volumetric ratio of 5:1 to 7:1 by continuous stirring using a magnetic stirrer, ii) mixing the above-said mixture with bovine serum albumin solution of strength ranging between 0.05-2% in a volumetric ratio of 1:3 to 1.5:3 under nitrogen atmosphere and stirring for 20 minutes by a magnetic stirrer, iii) heating the above resultant solution at a temperature in the range of 60-75°C for a period of 18-24 hours under nitrogen atmosphere to obtain calcium load 2-4 hours into alkaline diammonium hydrogen phosphite solution of strength 0,14-0.16 M, at a temperature ranging v) washing the above-soaked protein gel with deionized water to remove ammonium nitrate formed as by-product and recovering the nanosized hydroxyapatite from the soaked protein gel by the known method as herein described.

Filing Date: 28-03-2002

Issue Date: 28-02-2005

Applicant: CSIR-National Metallurgical Laboratory (CSIR-NML), Jamshedpur

Patent No: IN192392

Application No: 0394DEL2002

Inventor(s): Sinha A, Nayar S, Agrawal A, Rao V, Rao Pr

IPC Classification: C01B25/00, A61K 31/00

Indian Classification: 55E4

Country: India

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